IPS15 3 Europe Pushing the Thermal Limit of

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IPS-15 -3 Europe Pushing the Thermal Limit of HMX Perforating Systems in Through-Tubing Gas

IPS-15 -3 Europe Pushing the Thermal Limit of HMX Perforating Systems in Through-Tubing Gas Wells Dominic Wong Regional TCP Manager – ESSA May 20, 2015

Introduction ▌Through-tubing perforating systems based on HMX explosive are commonly deployed for gas well

Introduction ▌Through-tubing perforating systems based on HMX explosive are commonly deployed for gas well perforating ▌Important to consider jobs above 360 F at depths around 15, 000 ft ▌Large body of operational data shows a typical transit time to be 1. 0 hr, with another 0. 5 hr for tie-in time and shooting. ▌Total time of 1. 5 hr is nearing the HMX thermal limit. © 2014 HALLIBURTON. ALL RIGHTS RESERVED. 2

Background © 2014 HALLIBURTON. ALL RIGHTS RESERVED. 3

Background © 2014 HALLIBURTON. ALL RIGHTS RESERVED. 3

Goal of this test program ▌ Determine thermal delay inside the perforating gun. ▌

Goal of this test program ▌ Determine thermal delay inside the perforating gun. ▌ Conduct tests to take advantage of the delay so that thermal limit of the HMX charges can be “pushed” as much as possible before requiring a switch to HNS. ▌ Determine the performance of the HMX charges as a function of temperature. ▌ This phase concentrated on charge performance in aluminum targets. Follow-on phases are underway for HMX detonators and detonating cord, as well as HMX charge performance in stressed rock. © 2014 HALLIBURTON. ALL RIGHTS RESERVED. 4

Experimental Setup for Simulated Gas Well ▌ First step was to measure thermal delay

Experimental Setup for Simulated Gas Well ▌ First step was to measure thermal delay inside 2 -in OD x 7 ft length gun ▌ Eleven thermocouples positioned at various locations ▌ Linear heating ramp programmed to match 1: 00 hr transit time © 2014 HALLIBURTON. ALL RIGHTS RESERVED. 5

Setup inside oven Thermocouple © 2014 HALLIBURTON. ALL RIGHTS RESERVED. 6

Setup inside oven Thermocouple © 2014 HALLIBURTON. ALL RIGHTS RESERVED. 6

Full set of temperature curves Thermal delay inside gun at 1. 5 hr ©

Full set of temperature curves Thermal delay inside gun at 1. 5 hr © 2014 HALLIBURTON. ALL RIGHTS RESERVED. 7

Thermal delay at center charge vs gas well temperature © 2014 HALLIBURTON. ALL RIGHTS

Thermal delay at center charge vs gas well temperature © 2014 HALLIBURTON. ALL RIGHTS RESERVED. 8

Shooting fixture Target Stack Detonator Section © 2014 HALLIBURTON. ALL RIGHTS RESERVED. Charge Section

Shooting fixture Target Stack Detonator Section © 2014 HALLIBURTON. ALL RIGHTS RESERVED. Charge Section Target Section 9

Two-step heating method used to thermally equate shooting fixture with actual gun system ▌

Two-step heating method used to thermally equate shooting fixture with actual gun system ▌ Necessary due to thermal difference between mass of shooting fixture and mass of gun ▌ Fixture was necessarily large for safety reasons when pushing the limit of HMX (which is also beyond the delta phase transition temperature) © 2014 HALLIBURTON. ALL RIGHTS RESERVED. 10

Simulated Gas Well With Perforating Gun Transit time 1: 05 hr 380 F Well

Simulated Gas Well With Perforating Gun Transit time 1: 05 hr 380 F Well temp profile Shooting time 0: 30 hr later A B Charge temp profile -1 -

Simulated Gas Well With Perforating Gun Shooting time 0: 30 hr later Transit time

Simulated Gas Well With Perforating Gun Shooting time 0: 30 hr later Transit time 1: 05 hr 380 F Well temp profile 2 A 1 B Charge temp profile -2 -

Simulated Gas Well With Perforating Gun Shooting Fixture Inside Oven temp Shooting time 0:

Simulated Gas Well With Perforating Gun Shooting Fixture Inside Oven temp Shooting time 0: 30 hr later Transit time 1: 05 hr C D Charge temp 380 F Well temp profile 2 A 1 B Charge temp profile -3 -

Simulated Gas Well With Perforating Gun Shooting Fixture Inside Oven temp C Shooting time

Simulated Gas Well With Perforating Gun Shooting Fixture Inside Oven temp C Shooting time 0: 30 hr later Transit time 1: 05 hr D Charge temp 380 F Well temp profile 2 A 4 1 3 B Charge temp profile -4 - 368 F

Simulated Gas Well With Perforating Gun Shooting Fixture Inside Oven temp C Shooting time

Simulated Gas Well With Perforating Gun Shooting Fixture Inside Oven temp C Shooting time 0: 30 hr later Transit time 1: 05 hr D Charge temp 380 F Well temp profile 2 A 4 1 3 B Charge temp profile 0. 002% decomposition -5 - 368 F

Simulated Gas Well With Perforating Gun Shooting Fixture Inside Oven temp C Shooting time

Simulated Gas Well With Perforating Gun Shooting Fixture Inside Oven temp C Shooting time 0: 30 hr later Transit time 1: 05 hr D Charge temp 380 F Well temp profile 2 A 4 1 368 F 3 B Charge temp profile 0. 010% decomposition -6 -

Results Gas Well Temp (F) Baseline 360 370 380 400 420 440 Temp at

Results Gas Well Temp (F) Baseline 360 370 380 400 420 440 Temp at Center Charge After Simulated Run (1 -hr RIH + 30 min to shoot) (F) Ambient 342 358 368 380 403 415 No. of High-Order Test Shots 20 6 6 6 5 of 6 Misfires or Low-Order Firing? None None Yes, 1 of 6 Low-order firing © 2014 HALLIBURTON. ALL RIGHTS RESERVED. 17 Penetration Average in Aluminum (in) 8. 0 7. 9 7. 7 7. 5 7. 8 7. 3

Conclusions ▌ For all simulated BHTs, there was a thermal delay in the interior

Conclusions ▌ For all simulated BHTs, there was a thermal delay in the interior of the gun § At the 1: 30 hr exposure, the temperature of the center charge was still cooler than BHT by 12 -25 F § By 2: 00 hr, however, the entire gun had essentially reached thermal equilibrium with the BHT ▌ The HMX limit for the gun can be pushed, however, this advantage must be taken within the 1: 30 hr timeframe ▌ At the 1: 30 hr time, the upper limit for charge all-fire was 420 F BHT § Important to note that the results from this test program are applicable to gas wells only § The heat transfer characteristics of oil wells will be different, thereby giving different thermal delays and correspondingly different charge response © 2014 HALLIBURTON. ALL RIGHTS RESERVED. 18

Thank You / Questions © 2014 HALLIBURTON. ALL RIGHTS RESERVED. 19

Thank You / Questions © 2014 HALLIBURTON. ALL RIGHTS RESERVED. 19