GAS TECHNOLOGY INSTITUTE Hydrogen Quality Sampling Apparatus HQSA

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GAS TECHNOLOGY INSTITUTE Hydrogen Quality Sampling Apparatus (HQSA) at 70 MPa > www. gastechnology.

GAS TECHNOLOGY INSTITUTE Hydrogen Quality Sampling Apparatus (HQSA) at 70 MPa > www. gastechnology. org

Hydrogen Quality Sampling Apparatus (HQSA)- Outline 1. 2. 3. 4. 5. Background/Need Design Criteria

Hydrogen Quality Sampling Apparatus (HQSA)- Outline 1. 2. 3. 4. 5. Background/Need Design Criteria Engineering/Design Process Fabrication Testing and Acceptance www. gastechnology. org

Gas Technology Institute > Independent Non-Profit R&D organization > Focus on Energy and Environmental

Gas Technology Institute > Independent Non-Profit R&D organization > Focus on Energy and Environmental Issues – Specializing in natural gas and hydrogen > Main Facility: 18 -acre Campus Near Chicago GTI’s Main Research Facility – Over 200, 000 ft 2 of laboratory space – 28 specialized laboratories and facilities > Staff of 250 – 70% scientists and engineers GTI’s Energy & Environmental Technology Center – 50 Ph. Ds, 11 licensed PEs www. gastechnology. org

Background/Need > Developed under contract with NREL > Guidance from ASTM D 03. 14

Background/Need > Developed under contract with NREL > Guidance from ASTM D 03. 14 - WK 5847 Standard Practice for Sampling of High Pressure Hydrogen and Related Fuel Cell Feed Gases > Standardized analytical and test procedures to sample and measure non-hydrogen constituents > Confirm that fueling stations meet fuel quality guidelines www. gastechnology. org

www. gastechnology. org

www. gastechnology. org

ASTM D 03. 14 WK 5847 Work Group Sample Collection Sampling Adaptor Containers Analytical

ASTM D 03. 14 WK 5847 Work Group Sample Collection Sampling Adaptor Containers Analytical Methods Dispenser End Users WK 5847 Key Components • • • Safe Data Collection Representative and Repeatable Data Collection Gas Phase Sampling vs. Particulate Sampling - Different Collection Methodologies Equipment Decontamination and Cross Contamination Issues Must support analytical methods in achieving detection limits specified by recognized SDOs like SAE J 2719. www. gastechnology. org

ASTM D 03. 14 - WK 5847 Participants > > > > > Eric

ASTM D 03. 14 - WK 5847 Participants > > > > > Eric Lee (Technical Contact - Gaseous Phase) Jim Ohi (Contract Manager) Dr. JP Hsu (Sampling Contract) Lou Lautman (Design & Fabrication Contract) Tony Estrada (Design HAZOP Support) Arun Chemburkar, PE (HAZOP Courtesy of PG&E) Robert Boyd (Technical Contact – Particulates) James Simnick Matt Forrest Mark Rossetto Lori Law Eric Fuller David Fish Welker Dr. Raul Dominguez Dr. Werner Bergman Sheral Arbuckle Bruce Gollob Chrysler LLC NREL Smart Chemistry GTI PG&E ERM BOC/Linde BP Daimler. Chrysler NRC NRC Engineering SCAQMD Consultant Ford Atlantic Analytical www. gastechnology. org

Design Criteria > > > Rated for 700 bar (10, 000 psig) sampling Downward

Design Criteria > > > Rated for 700 bar (10, 000 psig) sampling Downward Compatible to 350 bar Universal for SAE J 2600 8 mm receptacle Non-Communication Design Trained Operator Conduct Hazard Analysis – Proper ratings – Overpressure protection – Safe discharge venting > Stay within budget www. gastechnology. org

Engineering/Design Process > Reviewed 350 bar device (CFCP) > Developed preliminary design > Reviewed

Engineering/Design Process > Reviewed 350 bar device (CFCP) > Developed preliminary design > Reviewed design with ASTM WG > Revised design and PID > Third-party conducted Hazard Analysis (May 2007) > Evaluated and incorporated HA results into final design > Final design approved www. gastechnology. org

Sampling Apparatus PID www. gastechnology. org

Sampling Apparatus PID www. gastechnology. org

Sampling Apparatus Design www. gastechnology. org

Sampling Apparatus Design www. gastechnology. org

Fabrication > > > Specified material compatibility Detailed BOM finalized Procured materials & fabricated

Fabrication > > > Specified material compatibility Detailed BOM finalized Procured materials & fabricated select components Assembled HQSA and portable vent/stand Drafted Operating Manual www. gastechnology. org

Operating Manual www. gastechnology. org

Operating Manual www. gastechnology. org

Testing & Acceptance > Leak test conducted in stages up to 88 MPa (12,

Testing & Acceptance > Leak test conducted in stages up to 88 MPa (12, 500 psig) > PRV actuation test & verification performed > Operating Manual drafted > Performance verification testing (at 350 bar) conducted > Samples safely captured > Operating Manual finalized > HQSA delivered > Field use being arranged www. gastechnology. org

Sampling Apparatus & Vent Stack www. gastechnology. org

Sampling Apparatus & Vent Stack www. gastechnology. org

Sampling Apparatus www. gastechnology. org

Sampling Apparatus www. gastechnology. org

Vent Stack www. gastechnology. org

Vent Stack www. gastechnology. org

Sampling Apparatus www. gastechnology. org

Sampling Apparatus www. gastechnology. org

Sampling Apparatus www. gastechnology. org

Sampling Apparatus www. gastechnology. org

Sampling Apparatus www. gastechnology. org

Sampling Apparatus www. gastechnology. org

70 MPa Sampling Apparatus www. gastechnology. org

70 MPa Sampling Apparatus www. gastechnology. org

Sampling Procedures www. gastechnology. org

Sampling Procedures www. gastechnology. org

Sampling Procedures > > > > > Verify regulator and vent valve settings Connect

Sampling Procedures > > > > > Verify regulator and vent valve settings Connect Dispenser Nozzle Initiate fill (test or manual mode may be required) Set sampling pressure regulator Set valves to flow hydrogen through sample cylinder to vent Operate valves to pressurize/purge cylinder 10 x Flow through cylinder to vent & prepare to collect Operate valves to capture sample Close Dispenser Nozzle valve and s/d Dispenser Depressurize HQSA then remove sample cylinder www. gastechnology. org

Sampling Apparatus PID www. gastechnology. org

Sampling Apparatus PID www. gastechnology. org

Tony Lindsay R&D Manager, Advanced Energy Systems Gas Technology Institute 1700 South Mount Prospect

Tony Lindsay R&D Manager, Advanced Energy Systems Gas Technology Institute 1700 South Mount Prospect Road Des Plaines, IL 60018 Phone: 847. 768. 0530 E-Mail: tony. lindsay@gastechnology. org Visit our website: www. gastechnology. org or www. gastechnology. org/hydrogen www. gastechnology. org