ZERTIFIKATE CERTIFICATE Certificaat SGS Environmental Services P O

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ZERTIFIKATE CERTIFICATE СЕРТИФИКАТ Certificaat

ZERTIFIKATE CERTIFICATE СЕРТИФИКАТ Certificaat

SGS Environmental Services P. O. Box 5252 NL-6802 EG Arnhem Tel : (+31) 26

SGS Environmental Services P. O. Box 5252 NL-6802 EG Arnhem Tel : (+31) 26 384 4500 Fax : (+31) 26 442 9410 VAT : NL 00 44 0 77 26 B 01 R. C. Rotterdam : 24226722 www. nl. sgs. com - REPORT - XMILE Europe B. V. Results of the emission measurements at the MS Catharina January 16 th 2013, baseline August 27 th 2014, with XMILE additive Project details General information Company name Address Postal code, city Contact Telephone number Email address Client reference number SGS reference number XMILE Europe B. V. Polderdijk 14 6914 KK Herwen Mr. M. Overbeeke (+31) (0) 6 47 57 04 83 marius@XMILE. eu MS Catharina EZMO/11/0027 -2 Plant details Location Plant Production details MS Catharina MAK 6 Mu 451 AK located Tolkamer, the Netherlands E 3 Test Cycle Measurement details Kind of measurement Measurement period Measuring staff Emission measurements, O 2, CO, NOx, PM January 16, 2013 and August 27, 2014 John van Middelkoop and Joop Kleverwal Signatures Project Manager Technical Manager Quality For a list of the accredited activities (Rv. A L 092) of the SGS Nederland BV Environmental Services Department in Arnhem, The Netherlands, we refer to the last three pages of the Dutch Accreditation Council Rv. A website (http: //www. rva. nl/? p=cins 0200). Disclaimer Unless agreed otherwise, all assignments are performed on the basis of the most recent version of the SGS Nederland BV General Terms and Conditions of Delivery. A simple request is all that is needed to have these terms and conditions sent to you again. We draw your attention to the limited liability, compensation and authorisation issues stipulated in these terms and conditions.

Intertek Nederland B. V Office/Laboratory Leerlooierstraat 135 3194 AB Hoogvliet Rt Tel. 010 -490

Intertek Nederland B. V Office/Laboratory Leerlooierstraat 135 3194 AB Hoogvliet Rt Tel. 010 -490 27 02 Xmile Europe B. V. Lichtenhorststraat 17 6942 GS Didam Netherlands Laboratory Report No. Postal address P. O. Box 575 3190 AM Hoogvliet Rt Fax 010 -472 32 25 Telex 62090 16 -015864 -0 -RDAM( 5) Date: Our Ref. : I 29438 Sample ID 16 -015864 -0 -RDAM-001 -00 Description Submitted sample: Tankstation Roto 1 Tank BV, Transvaal 50, 4254 BC Sleeuwijk 18 -OCT-2016 Product Gasoline XMILE EURO 95 Seals None Packing Plastic (> 250 ml) Test Method Specification Result R. O. N. ISO 5164 min. 95. 0 95. 4 M. O. N. ISO 5163 min. 85. 0 85. 1 Lead EN 237 mg/l max 5. 0 <2. 5 Manganese EN 16135 mg/l max. 2. 0 <2. 0 Density at 15 o. C ISO 12185 kg/m 3 720 -775 728. 9 Sulphur ISO 20846 mg/kg max. 10 5. 3 Induction Period at 100 o. C ISO 7536 min 360 >480 Gum content (Solvent-washed) ISO 6246 mg/100 ml max. 5 <1 Copper Corrosion 3 hrs. at 50 o. C ISO 2160 max. 1 1 A Appearance Visual Clear and bright Olefins ISO 22854 %v max. 18. 0 9. 2 Aromatics ISO 22854 %v max. 35. 0 24. 4 Benzene ISO 22854 %v max. 1. 00 0. 67 Oxygen content EN 22854 %m max. 2. 7 2. 41 Oxygenates EN 22854 Methanol %v max. 3. 0 <0. 01 Ethanol %v max. 5. 0 4. 65 Isopropyl alcohol %v <0. 01 Isobutyl alcohol %v <0. 01 Tert-butyl alcohol %v <0. 01 Ethers (5 or more C-atoms) %v 3. 5 Other oxygenates %v <0. 1 Laboratory Report No. Unit 24 -OCT-2016 16 -015864 -0 -RDAM( 5) Page 1 of 2 Precision complies with the reference method. The analytical report is issued in the name and for account of the principal who recognizes that this report purely represents the situation at a given moment. The principal commits himself to disclose each time the complete report and not parts of the report. Fax and E-mail copies have no legal force. The report can only be used within the specific context of the order and is only valid for the samples and for the company that gave the order. All relations between Intertek Nederland B. V. and its Principals will be governed by the latest version of the General Conditions of Intertek Nederland B. V. , filed of record with the Registry of the District Court at Rotterdam, which will be forwarded free of charge upon first request. Intertek Nederland B. V. explicitly rejects applicability of any general conditions applied by it’s Principals.

Intertek Nederland B. V Test Method Unit Specification Result Vapour Pressure EN 13016 -1

Intertek Nederland B. V Test Method Unit Specification Result Vapour Pressure EN 13016 -1 k. Pa 65. 0 -95. 0 84. 9 Distillation ISO 3405 IBP o. C Evap. at 70 o. C %v 22. 0 -50. 0 42. 9 Evap. at 100 oc %v 46. 0 -71. 0 62. 9 Evap. at 150 o. C %v min. 75. 0 92. 4 F. B. P. o. C max. 210 179. 8 Residue %v max. 2 1. 0 Loss %v Vapour Lock Index EN 228 25. 8 1. 5 Max. 1214 1150 Product meets EN 228 Class E 1 Sample Analysed : 24 -OCT-2016 XMILE EURO 9 S ( xmile gasoline ) Meets EUROPEAN STANDARD: EN 228 Laboratory Report No. 16 -015864 -0 -RDAM( 5) Page 2 of 2 Precision complies with the reference method. The analytical report is issued in the name and for account of the principal who recognizes that this report purely represents the situation at a given moment. The principal commits himself to disclose each time the complete report and not parts of the report. Fax and E-mail copies have no legal force. The report can only be used within the specific context of the order and is only valid for the samples and for the company that gave the order. All relations between Intertek Nederland B. V. and its Principals will be governed by the latest version of the General Conditions of Intertek Nederland B. V. , filed of record with the Registry of the District Court at Rotterdam, which will be forwarded free of charge upon first request. Intertek Nederland B. V. explicitly rejects applicability of any general conditions applied by it’s Principals.

Intertek Nederland B. V Office/Laboratory Leerlooierstraat 135 3194 AB Hoogvliet Rt Tel. 010 -490

Intertek Nederland B. V Office/Laboratory Leerlooierstraat 135 3194 AB Hoogvliet Rt Tel. 010 -490 27 02 Xmile Europe B. V. Lichtenhorststraat 17 6942 GS Didam Netherlands Postal address P. O. Box 575 3190 AM Hoogvliet Rt Fax 010 -472 32 25 Telex 62090 Laboratory Report No. 16 -015865 -0 -RDAM( 5) Date: Our Ref. : I 29438 24 -OCT-2016 Sample ID 16 -015865 -0 -RDAM-001 -00 Description Submitted sample: Tankstation i. Fuel Aleven, Nobelstraat 5, 6902 PH Zevenaar 18 -OCT-2016 Product XMILE Diesel Seals None Packing Plastic (> 250 ml) Test Method Unit Specification Result Flashpoint ISO 2719 o. C Above 55 66. 0 Conradson Carbon Residue on 10% v. ISO 10370 %m max. 0. 30 <0. 10 Water ISO 12937 mg/kg max. 200 60 Ash ISO 6245 %m max. 0. 01 <0. 01 Contamination EN 12662 mg/kg max. 24 <12 Copper Corrosion 3 hrs. at 50 o. C ISO 2160 class 1 1 A Oxidation Stability EN 12205 g/m 3 max. 25 <1 Lubricity ISO 12156 -1 micrometer max. 460 356 Sulphur ISO 20846 mg/kg max. 10 7. 8 Cloudpoint ASTM D 5771 o. C Cold Filter Plugging Point EN 116 o. C max. -5 -15 Density at 15 o. C ISO 12185 kg/m 3 820 -845 835. 6 Viscosity at 40 o. C ISO 3104 mm 2/s 2. 00 - 4. 50 3. 107 Cetane Number (DCN) EN 15195 min. 51. 0 53. 6 Cetane Index ISO 4264 min 46. 0 56. 3 Distillation ISO 3405 -2. 3 Rec. at 250 o. C %v max. 65. 0 24. 2 Rec. at 350 o. C %v min. 85. 0 94. 1 95 % v/v rec. at o. C 353. 9 Polycyclic Aromatics Hydrocarbons EN 12916 %m max. 8 2. 1 F. A. M. E EN 14078 %v max. 7. 0 5. 67 Manganese EN 16576 mg/l max. 2. 0 <0. 5 Laboratory Report No. 16 -015865 -0 -RDAM( 5) Page 1 of 2 Precision complies with the reference method. The analytical report is issued in the name and for account of the principal who recognizes that this report purely represents the situation at a given moment. The principal commits himself to disclose each time the complete report and not parts of the report. Fax and E-mail copies have no legal force. The report can only be used within the specific context of the order and is only valid for the samples and for the company that gave the order. All relations between Intertek Nederland B. V. and its Principals will be governed by the latest version of the General Conditions of Intertek Nederland B. V. , filed of record with the Registry of the District Court at Rotterdam, which will be forwarded free of charge upon first request. Intertek Nederland B. V. explicitly rejects applicability of any general conditions applied by it’s Principals.

Intertek Nederland B. V Test Method Conductivity ASTM D 2624 Unit Measuring Temperature o.

Intertek Nederland B. V Test Method Conductivity ASTM D 2624 Unit Measuring Temperature o. C Conductivity p. S/m Specification Result 23. 0 351 min. 150 Product meets EN 590 Class C Sample Analysed : 24 -OCT-2016 XMILE DIESEL Meets EUROPEAN STANDARD: Laboratory Report No. 16 -015865 -0 -RDAM( 5) EN 590 Page 2 of 2 Precision complies with the reference method. The analytical report is issued in the name and for account of the principal who recognizes that this report purely represents the situation at a given moment. The principal commits himself to disclose each time the complete report and not parts of the report. Fax and E-mail copies have no legal force. The report can only be used within the specific context of the order and is only valid for the samples and for the company that gave the order. All relations between Intertek Nederland B. V. and its Principals will be governed by the latest version of the General Conditions of Intertek Nederland B. V. , filed of record with the Registry of the District Court at Rotterdam, which will be forwarded free of charge upon first request. Intertek Nederland B. V. explicitly rejects applicability of any general conditions applied by it’s Principals.

Intertek Nederland B. V Office/Laboratory Leerlooierstraat 135 3194 AB Hoogvliet Rt Tel. 010 -490

Intertek Nederland B. V Office/Laboratory Leerlooierstraat 135 3194 AB Hoogvliet Rt Tel. 010 -490 27 02 Xmile Europe B. V. Lichtenhorststraat 17 6942 GS Didam Netherlands Laboratory Report No. Postal address P. O. Box 575 3190 AM Hoogvliet Rt Fax 010 -472 32 25 Telex 62090 16 -015864 -0 -RDAM( 5) Date: Our Ref. : I 29438 Sample ID 16 -015864 -0 -RDAM-001 -00 Description Submitted sample: Tankstation Roto 1 Tank BV, Transvaal 50, 4254 BC Sleeuwijk 18 -OCT-2016 Product Gasoline XMILE EURO 95 Seals None Packing Plastic (> 250 ml) Test Method Specification Result R. O. N. ISO 5164 min. 95. 0 95. 4 M. O. N. ISO 5163 min. 85. 0 85. 1 Lead EN 237 mg/l max 5. 0 <2. 5 Manganese EN 16135 mg/l max. 2. 0 <2. 0 Density at 15 o. C ISO 12185 kg/m 3 720 -775 728. 9 Sulphur ISO 20846 mg/kg max. 10 5. 3 Induction Period at 100 o. C ISO 7536 min 360 Gum content (Solvent-washed) ISO 6246 mg/100 ml max. 5 Copper Corrosion 3 hrs. at 50 o. C ISO 2160 max. 1 Appearance Visual Clear and bright Olefins ISO 22854 Aromatics ISO 22854 Method ISO 22854 1 EN 13016 EN 05 22854 ISO 34 EN 22854 Unit 24 -OCT-2016 %v Unit % v k. Pa % v Benzene Test Oxygen content %m e our Pressur Vap. Oxygenates o. C tillation Dis. Methanol %v%v P v IBEthanol %%v p. at 70 o. C v Eva % Isopropyl alcohol %v 0 oc vap. at 10 alcohol EIsobutyl o. C %v o. C vap. at 150 alcohol ETert-butyl v % %v. B. P. v FEthers % (5 or more C-atoms) %v idue es R Other oxygenates %v EN 228 Loss ock Index Vapour L 1 8 Class E 16 eets EN 22 4 -OCT-20 Laboratory 5) Product m Reportse. No. d : 216 -015864 -0 -RDAM( max. on 18. 0 Specificati max. 35. 0 0 5. 65. 0 -9 max. 1. 00 max. 2. 7 22. 0 -50. 0 -71. 3. 0 46 max. . 0 5. 0 in. 75 mmax. 0 21. ax m max. 2 Max. 1214 >480. V ederland B Intertek N <1 1 A Clear and bright Result 9. 2 84. 9 24. 4 0. 67 25. 82. 41 42. 9 62. 9 <0. 01 92. 4 4. 65 179. 8 <0. 01 1. 0 <0. 01 1. 5 <0. 01 1150 3. 5 <0. 1 ) gasoline. Page e il of 2 1 m x ( S 9 naly ILE EURO s Sample A t M e X e M Precision complies with the reference method. The analytical report is issued in the name and for account of the principal who recognizes that this report EN 228 purely represents the situation at a given moment. The principal commits himself to disclose each time the complete report and not parts of the report. Fax and E-mail copies have no legal force. The report can only be used within the specific context of the order and is only valid for the samples and for the company that gave the order. All relations between Intertek Nederland B. V. and its Principals will be governed by the latest version of the General Conditions of Intertek Nederland B. V. , filed of record with the Registry of the District Court at Rotterdam, which will be forwarded free of charge upon first request. Intertek Nederland B. V. explicitly rejects applicability of any general conditions applied by it’s Principals. EU TAND AR RO PEAN S D:

Intertek Nederland B. V Office/Laboratory Leerlooierstraat 135 3194 AB Hoogvliet Rt Tel. 010 -490

Intertek Nederland B. V Office/Laboratory Leerlooierstraat 135 3194 AB Hoogvliet Rt Tel. 010 -490 27 02 Xmile Europe B. V. Lichtenhorststraat 17 6942 GS Didam Netherlands Postal address P. O. Box 575 3190 AM Hoogvliet Rt Fax 010 -472 32 25 Telex 62090 Laboratory Report No. 16 -015865 -0 -RDAM( 5) Our Ref. : I 29438 24 -OCT-2016 Sample ID 16 -015865 -0 -RDAM-001 -00 Description Submitted sample: Tankstation i. Fuel Aleven, Nobelstraat 5, 6902 PH Zevenaar 18 -OCT-2016 Product XMILE Diesel Seals None Packing Plastic (> 250 ml) Date: Test Method Unit Specification Result Flashpoint Conradson Carbon Residue on 10% v. Water ISO 2719 ISO 10370 ISO 12937 o. C %m mg/kg Above 55 max. 0. 30 max. 200 66. 0 <0. 10 60 Ash Contamination Copper Corrosion 3 hrs. at 50 o. C ISO 6245 EN 12662 ISO 2160 %m mg/kg max. 0. 01 max. 24 class 1 <0. 01 <12 1 A Oxidation Stability Lubricity Sulphur Cloudpoint EN 12205 ISO 12156 -1 ISO 20846 ASTM D 5771 g/m 3 micrometer mg/kg o. C max. 25 max. 460 max. 10 <1 356 7. 8 -2. 3 Cold Filter Plugging Point Density at 15 o. C Viscosity at 40 o. C EN 116 ISO 12185 ISO 3104 o. C kg/m 3 mm 2/s Cetane Number (DCN) Cetane Index Distillation EN 15195 ISO 4264 ISO 3405 Rec. at 250 o. C min. 51. 0 min 46. 0 53. 6 56. 3 %v max. 65. 0 24. 2 min. 85. 0 94. 1 max. 8 max. 7. 0 353. 9 2. 1 5. 67 Rec. at 350 o. C Polycyclic Aromatics Hydrocarbons 95 % v/v rec. at F. A. M. E EN 12916 EN 14078 % v % o. Cm %v Manganese EN 16576 mg/l 2016 O C T- ass 90 Cl E N 5 d : 24 s t e e e ct m Analys. No. Laboratory 16 -015865 -0 -RDAM( Produ ple Report m a S C 5) d B. V lan max. -5 -15 Neder ertek t n I 820 -845 835. 6 2. 00 - 4. 50 3. 107 XMILEmax. 2. 0 L D IE S E s M eet <0. 5 Page 1 of 2 Precision complies with the reference method. The analytical report is issued in the name and for account of the principal who recognizes that this report purely represents the situation at a given moment. The principal commits himself to disclose each time the complete report and not parts of the report. Fax and E-mail copies have no legal force. The report can only be used within the specific context of the order and is only valid for the samples and for the company that gave the order. All relations between Intertek Nederland B. V. and its Principals will be governed by the latest version of the General Conditions of Intertek Nederland B. V. , filed of record with the Registry of the District Court at Rotterdam, which will be forwarded free of charge upon first request. Intertek Nederland B. V. explicitly rejects applicability of any general conditions applied by it’s Principals.

CERTIFICATE

CERTIFICATE

ZERTIFIKATE CERTIFICATE

ZERTIFIKATE CERTIFICATE