Nuclear Magnetic Resonance ANIMATED ILLUSTRATIONS MS Powerpoint Presentation

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Nuclear Magnetic Resonance ANIMATED ILLUSTRATIONS MS Powerpoint Presentation Files Uses Animation Schemes as available

Nuclear Magnetic Resonance ANIMATED ILLUSTRATIONS MS Powerpoint Presentation Files Uses Animation Schemes as available in MS XP or MS 2003 versions A class room educational material File-4 Principles of NMR signal detection: NMR Spectrum http: //ugc-inno-nehu. com/links_from_web. html

Oscillation Level reduced when there is ESR absorption Oscillation Level at fixed frequency ‘ν’

Oscillation Level reduced when there is ESR absorption Oscillation Level at fixed frequency ‘ν’ When No ESR Detected DC Level No ESR 2 Oscillator Φ Oscillation Level Detector 1 Reduced DC On ESR Absorption Shifter hν=gβH No oscillations 0 The role of a phase Φ shifter in the diagram would be explained in the succeeding slides If the Current is increased from 0 to beyond resonance field, then, the field [ Ht ] increases with time and causes resonance at resonance field value Ht hν=gβH 2 Current Source CLICK to transit to next slide 1

Z - Magnetization along the Field XY - Magnetization induces RF signal in the

Z - Magnetization along the Field XY - Magnetization induces RF signal in the receiver coil Z Defocusing and signal decay Y X Output from receiver coil - FID RF Pulse : π/2 pulse to flips the magnetization into xy plane CW Oscillator GATE Receiverdetector RF Pulse DC Pulse generator Probe In Magnet Display Monitor Recorder

Real imaginary OUTPUT from the FFT Program: Time domain FID and the Frequency domain

Real imaginary OUTPUT from the FFT Program: Time domain FID and the Frequency domain two line NMR spectrum

Spectrometer operating frequency decreases Distance of separation between the multiplets varies with the field

Spectrometer operating frequency decreases Distance of separation between the multiplets varies with the field Field= H Separation within the multiplets remain unchanged with the field H/2 H/4 H/6. 6