Ne SSI New SamplingSensor Initiative 2001 Spring Sponsor

Ne. SSI (New Sampling/Sensor Initiative) 2001 Spring Sponsor Meeting Center for Process Analytical Chemistry New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

Agenda • Status and Update - PV 2 Introduction (Why CPAC) What is Ne. SSI What has happened/is happening • Ne. SSI Team Goals - Rdubois • Bluetooth - Mike Horton (Crossbow) • Connectivity - PV 2 New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

CPAC as a Multi-Purpose PA Forum • Legal Umbrella for Sponsors to Meet R&D: Long Range / Short Range Information Clearing House Enabling Mechanism to Address Other Common Needs • Focus Groups: Forum to Review R&D Programs Present Industry Common Needs - RFP Address Other Industry Common Needs Fieldbus Datalink Specification - Done Ne. SSI /Micro-Reactor Analytics - In progress Chemometrics On-line/Connectivity - Future? New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

What is Ne. SSI? • Adapt Modular Surface Mount Technology from the SEMI Industry to Sampling System Design in the Chemical Industry • Driving Forces for Change Cost to Build/ Cost of Ownership Traditional Sampling System Designs Same for Last 20+ Years Weak Link in Overall Analyzer Reliability Integrate Other Sensors (Smart Sampling System) Sample Validation New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

What is Ne. SSI? Picture courtesy Swagelok® New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

What is Ne. SSI? New 5 Channel Design by Parker Picture courtesy Parker New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

What is Ne. SSI? - It is SMART Legend: P Pressure Sensor T Temp Sensor V Valve A Analytical Sensor New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

Ne. SSI Vision (Now) New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

Ne. SSI Vision (Next Step) Signal Wires Only V T P Sensor Analytical Manager (SAM) A Shared Power Bus New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001 Signal to AC

Background and Chronology of Ne. SSI Activities • Oil&Petrochemical (O&P) Focus Group May 1999 Identified Sampling Systems as Common Area Of Interest Sponsored Tutorial for Nov 99 Sponsor Meeting • Tutorial Nov 99 CPAC Meeting Background/Reasons for Interest Presentations by Suppliers/ End Users • Participation in IFPAC 2000 Meeting Plenary/General Papers (SS Enjoyed High Profile) Workshop New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

Background and Chronology of Ne. SSI Activities (cnt’d) • Ad-hoc O&P Meeting @ Pittcon 2000 End-users Discuss Initial Target Designs • CPAC 2000 Spring Meeting Formed SS Focus Group Defined Information Package (basis of RFP) • Distributed Request for Proposal (RFP) (July 2000) Clarification Meeting at ISAEXPO 2000 (40 attendees) Received Proposals/Feedback from Swagelok, Parker, Autoflow, ABB Analytical, SAAI, Rosemount Analytical New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

Background and Chronology of Ne. SSI Activities (cnt’d) • CPAC 2000 Fall Meeting Previewed Swagelok/Parker Proposals Micro-Reactor Proposal (Micro-Analytics) Planning (CD Deliverable, IFPAC 2001, Pittcon etc. ) • IFPAC 2001 Sampling System Session at IFPAC 2001 Review and Summary of Ne. SSI Effort (RD/PV 2) Papers by Swagelok, Parker, Autoflow, ABB, Rosemount Ad-hoc Meeting (Standing Room only Interest) New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

Background and Chronology of Ne. SSI Activities (cnt’d) • Pittcon 2000 Meeting Ne. SSI Ad-hoc Forum Meeting Confirmed viability of Ne. SSI designs Introduced the Role of Wireless (Bluetooth) Focus on Special Issues/Problems Swagelok, Parker, ABB Highlighted Special Problems 4 Subteams (Intrinsic Safety, Component availability etc. ) • Miscellaneous/In the Pipeline Proposal for Additional Resource Jim Tatera (retiree from Dow Corning) Part-time to lead key sub-team activities Deliverables/schedule defined Report at next CPAC Meeting (Nov) More details of proposal etc. at SSFG (Wednesday) New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

Background and Chronology of Ne. SSI Activities (cnt’d) • Miscellaneous/In the Pipeline (cnt’d) Testing/Evaluation Two Systems in Design Phase (EMCC) Rosemount Laboratory Tests Completed (see SSFG) Test System Available More Participation by End-users needed Ne. SSI Deliverable Completed CD Issued Ne. SSI Website Up-to-date Ne. SSI Promotional efforts Distribution List > 150 names Present Hour Tutorial at ISA 2001 Meeting (Sept 01) Globalization efforts CPACT Presentation Apr 01 (high interest, additional names) Paper tentatively accepted for INTERMAC Meeting (Nov 01) Extending SP 76 to IEC standard New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

Acknowledgements • Dow Ron O’Reily/Brian Worthington/Walter Henslee • Dow Corning Jim Tatera. J/Gary Bokerman. J • Du. Pont Joe Adrisani, Chuck Miller, Bob Bucher, Bruce Johnson • Rohm&Haas Joe Sung • Honeywell Ken Creasy, Ullrich Bonne, Troy Francisco • Exxon. Mobil Dan Podkulski/Rajko Puzic/Paul Hromadka/John Cumbus/Jeff Gunnell • Swagelok Dave Simko/Rick Ales & Colleagues • Parker Steve Doe, Frank Ruiz & Colleagues • Rosemount John Gajewski & Colleagues • Thermo. Onix Jerry Evans • CPAC Lloyd Burgess/Larry Ricker • Others ABB, Panametrics, AAI, Sterling Chemicals New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

…. and they lived happily ever after FINI New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

O&P Focus Group Meeting May 99 • Recognized Modular Sampling System Efforts in Semi Conductor Industry (Standard) • Vendors like Autoflow, A+, Swagelok etc. promoted modular designs • Recognized that current implementations of sample systems designs have not changed for many years • CPAC has promoted Versatile Micro Analytical Systems (VMAS) as a basis for future micro-analytical techniques • O&P decided to sponsor a SSISSS (Small Smart Integrated Sensor and Sampling System) Tutorial at CPAC Nov Meeting New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

Nov 99 CPAC SSISSS Tutorial • Exxon. Mobil/Du. Pont Provided Introduction to Tutorial Validation of Sample System Performance Integration of Sensor with Sampling System • Four Suppliers of Sampling/Analyzer Systems Participated in Tutorial: A+, Autoflow, Swagelok, Rosemount Many components commercially Available GCX example of self-contained miniaturized GC (GC on a pole) • Recognition Modular Sampling System can be a platform to integrate VMAS Bridge between Process Sample (Macro world) Micro Fluidics Sensors/Analyzers New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

Driving Forces for Change • Reduce Cost of Ownership Non Recurring Costs = Cost to Build Operating Cost • Data Validation (Fit for Use) New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

Integration of Sample System and Sensors All System Components in Contact with Sample including the Sensors Sample Conditioning System Process Stream New Sampling/Sensor Initiative (Ne. SSI) Field LAN A Mainly a Trust Configuration Now a Trust & Verify Configuration P T F Level 0 Analyzer Controller All Additional Electronic and Computing Components Required to Generate Analytical Result Level 1 CPAC: May 7, 2001

Level 0 Subsystem Integration Purpose: Prepare and Verify a Representative Sample (Compatible with Analyzer Sensor) Sample Conditioning System Integrated Sampling/Sensor System Process Stream A New Sampling/Sensor Initiative (Ne. SSI) P Opportunity: T • Size • Cost F Level 0 Packaging as an Integrated Sensor and Sampling System Issues: • Size • Standardization • VMAS CPAC: May 7, 2001

Separation or Integration of Level 0/1 Subsystems Objective: Close to Sample Tap Field LAN Integrated Sampling/Sensor System Process Stream A P T F Analyzer Controller Options: • Remote • Separate but Close • Integrated New Sampling/Sensor Initiative (Ne. SSI) Level 0 Level 1 CPAC: May 7, 2001

Integration of Level 0/1 Subsystems Integrated Sampling/Sensor/Controller System Process Stream Field LAN A P $$ T Analyzer Controller F New Sampling/Sensor Initiative (Ne. SSI) Level 0 Level 1 CPAC: May 7, 2001

Nov 99 CPAC SSISSS Tutorial • Exxon. Mobil/Du. Pont Provided Introduction to Tutorial Validation of Sample System Performance Integration of Sensor with Sampling System • Four Suppliers of Sampling/Analyzer Systems Participated in Tutorial: A+, Autoflow, Swagelok, Rosemount Many components commercially Available GCX example of self-contained miniaturized GC (GC on a pole) • Recognition Modular Sampling System can be a platform to integrate VMAS Bridge between Process Sample (Macro world) Micro Fluidics Sensors/Analyzers New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

Nov 99 CPAC SSISSS Tutorial (Vendor Presentations) Swagelok Autoflow A+ New Sampling/Sensor Initiative (Ne. SSI) Rosemount CPAC: May 7, 2001

Nov 99 CPAC SSISSS Tutorial • Exxon. Mobil/Du. Pont Provided Introduction to Tutorial Validation of Sample System Performance Integration of Sensor with Sampling System • Four Suppliers of Sampling/Analyzer Systems Participated in Tutorial: A+, Autoflow, Swagelok, Rosemount Many components commercially Available GCX example of self-contained miniaturized GC (GC on a pole) • Recognition Modular Sampling System can be a platform to integrate VMAS Bridge between Process Sample (Macro world) and Micro Fluidics Sensors/Analyzers New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

IFPAC 2000 • Exxon. Mobil Presented Plenary Paper Promoting SSISSS Sample System Infrastructure accounts for 50+% Cost to Build Proposed Conceptual Design for SSISSS Highlighted sensor and analyzer transmitter configurations • Sampling System Session Presentations by A+, Autoflow, etc. Sampling Systems enjoyed a High Profile • CPAC/Exxon. Mobil sponsored Workshop Confirmed high interest in Modular Sampling System Provided input for the ISA Standardization effort New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

TODAY’S COST OF BUILD For a major greenfield project New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

TODAY’S COST OF OWNERSHIP New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

IMAGINE THE FUTURE P T Analyzer Controller F Level 0 New Sampling/Sensor Initiative (Ne. SSI) Field LAN Process Stream A Level 1 CPAC: May 7, 2001

IMAGINE THE FUTURE FLAN (Optical Fiber) Sensor = Moisture Probe P T F A IA Controller (ASIC) & Interface Module Sensor/Signal Bus Original Picture of Gas Delivery System courtesy Valin Corporation; New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

IMAGINE THE FUTURE Sensor = RAMAN Probe P T F Interface Module A New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

IFPAC 2000 • Exxon. Mobil Presented Plenary Paper Promoting SSISSS Sample System Infrastructure accounts for 50+% Cost to Build Proposed Conceptual Design fro SSISSS Highlighted sensor and analyzer transmitter configurations • Sampling System Session Presentations by A+, Autoflow, etc. Sampling Systems enjoyed a High Profile • CPAC/Exxon. Mobil sponsored Workshop Confirmed high interest in Modular Sampling System Provided input for the ISA Standardization effort New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

IFPAC 2000 • Exxon. Mobil Presented Plenary Paper Promoting SSISSS Sample System Infrastructure accounts for 50+% Cost to Build Proposed Conceptual Design fro SSISSS Highlighted sensor and analyzer transmitter configurations • Sampling System Session Presentations by A+, Autoflow, etc. Sampling Systems enjoyed a High Profile • CPAC/Exxon. Mobil sponsored Workshop Confirmed high interest in Modular Sampling System Provided input for the ISA Standardization effort New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

Pittcon 2000 (New Orleans) • O&P Ad-Hoc Meeting of Sponsor End-users Du. Pont, Dow-Corning, CPAC, Rohm&Haas, Exxon. Mobil • Main Goal: Identify Typical Sample System Designs as Candidates for Modular Design Reviewed some typical gas/liquid sample System Designs Rob Du. Bois Presented a Modular Component/Service Matrix • Discussed next steps Present Sample System Data at May CPAC Meeting Next Step is to Open Up Discussion (3 rd parties) Leverage ISA Meeting in New Orleans (Aug 00) • Role of CPAC in Facilitating Development/Testing of a Prototype System Larry Ricker/Lloyd Burgess to Present Proposal New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001

Status • CPAC Meeting May 1999 Done O&P Identified Modular Sampling Systems • CPAC Meeting Nov 1999 Done O&P Sponsored Tutorial • IFPAC 2000 Meeting Done Plenary Presentation Promoted SSISS Session on Modular Sampling Systems CPAC Sponsored Workshop • Pittcon 2000 Done Ad-hoc O&P Meeting Propose Candidate Sampling System Descriptions • CPAC Meeting May 2000 New Sampling/Sensor Initiative (Ne. SSI) TBD CPAC: May 7, 2001

What is Next? • CPAC Meeting May 2000 (Sampling Focus Group – Wednesday) Review and Agree on Sample System Information Package Involvement of 3 rd parties How do we distribute package (Distribution List, Meeting? ) Expectations for proposals from Suppliers (Paper designs? ) Joint Effort with ISA (Meeting in Aug, New Orleans) Evaluation of Designs - Recommendation • Prototype design/manufacturing/testing at CPAC Larry Ricker/Lloyd Burgess proposal • Program to Evaluate Test Platforms fro Micro Analytical Devices CPAC Proposal – Lloyd Burgess New Sampling/Sensor Initiative (Ne. SSI) CPAC: May 7, 2001