Beryllium and graphite capsule design progress update Kavin

Beryllium and graphite capsule design progress update Kavin Ammigan BNL BLIP Irradiation Planning Meeting VC 6 17 October 2016

Beryllium Capsule SS 304 L capsule drawing being finalized v Capsule atmosphere: Argon v Total specimen thickness: 9. 5 mm PF-60, S-200 FH, S-65 F Hi. Rad. Mat specimens ordered PF-60, S-65 F, UHP microstructural specimens ordered S 65 F & PF 60 bend bars ordered S-65 F & PF-60 tensile specimens ordered 0. 009” SS 304 L sheet ordered 2 2/28/2021 K. Ammigan | Beryllium and graphite capsule design progress update Graphite outer filler drawings being finalized

PIE Plans - Beryllium Specimen Bend Tensile Hi. Rad. Mat Microstructural Side filler Outer side filler Outer top/bottom filler Capsule Window 3 2/28/2021 Quantity to Cool-down Shipping Shipment Disposal at BNL Grade Quantity be tested time (mo) PIE location (Y/N) by (Y/N) PIE tests PF-60 24 16 ≥ 3 PNNL Y Oct-17 N Bend, CTE, microstructural S-65 F 24 16 ≥ 3 PNNL Y Oct-17 N Bend, CTE, microstructural PF-60 24 16 ≥ 3 PNNL Y Oct-17 N Tensile S-65 F 24 16 ≥ 3 PNNL Y Oct-17 N Tensile PF-60 8 2 ≥ 3 CERN Y Dec-17 N In-beam thermal shock S-65 F 8 2 ≥ 3 CERN Y Dec-17 N In-beam thermal shock S-200 FH 8 2 ≥ 3 CERN Y Dec-17 N In-beam thermal shock PF-60 4 3 ≥ 3 Oxford/CCFE Y Oct-17 N Microstructural analysis S-65 F 5 3 ≥ 3 Oxford/CCFE Y Oct-17 N Microstructural analysis UHP 1 1 ≥ 3 Oxford/CCFE Y N Microstructural analysis ZXF-5 Q 4 ≥ 3 N/A N N/A Y N/A ZXF-5 Q 2 ≥ 3 N/A N N/A Y N/A SS 304 1 ≥ 3 N/A N N/A Y N/A SS 304 2 ≥ 3 N/A N N/A Y N/A K. Ammigan | Beryllium and graphite capsule design progress update

Graphite Capsule v Capsule atmosphere: Vacuum v Total specimen thickness: 5. 5 mm SS 304 L capsule drawing being finalized IG-430, ZXF-5 Q tensile specimens in fabrication IG-430, ZXF-5 Q, GC 20 Hi. Rad. Mat specimens in fabrication 0. 009” SS 304 L window ordered 3 D C/C CTE specimens in fabrication GC 20, IG-430, ZXF-5 Q bend bars in fabrication 4 2/28/2021 K. Ammigan | Beryllium and graphite capsule design progress update Outer filler drawings being finalized

PIE Plans - Graphite Specimen Bend Grade Quantity Cool. PIE Shipping Shipment to be down location (Y/N) by tested time (mo) ZXF-5 Q IG-430 GC 20 12 12 12 2 6 6 6 2 2 2 ≥ 3 ≥ 3 ≥ 3 PNNL BNL BNL Y Y Y N N N Oct-17 N/A N/A Tensile ZXF-5 Q 7 4 ≥ 3 BNL N N/A Hi. Rad. Mat CTE Side filler Outer side filler Outer top/bottom filler Capsule Window IG-430 ZXF-5 Q IG-430 GC 20 3 D C/C ZXF-5 Q 7 5 5 6 6 2 2 4 - ≥ 3 ≥ 3 ≥ 3 BNL CERN BNL N/A N Y Y Y N N N N/A Dec-17 N/A ZXF-5 Q SS 304 2 1 2 - ≥ 3 ≥ 3 N/A N/A N/A 5 2/28/2021 3 3 2 4 - Disposal at BNL (Y/N) PIE tests Bend, microstructural CTE CTE Tensile, ultrasonic Y - after testing measurement N In-beam thermal shock Y - after testing CTE measurement Y - after cool-down N/A N N N Y - after testing Y - after cool-down N/A K. Ammigan | Beryllium and graphite capsule design progress update

Next steps • Finalize SS capsule and outer filler drawings and begin fabrication • Update capsule thermal analyses • Coordinate activities with BNL and EB industries for capsule welding 6 2/28/2021 K. Ammigan | Beryllium and graphite capsule design progress update