1 H NMR Hexane C 6 H 14

1 H NMR

Hexane (C 6 H 14 ) Assign. Shift (ppm) A 1. 29 B 1. 27 C 0. 89 J(A, C) = 6. 9 HZ. 89. 56 MHz (CDCl 3)

Octane (C 8 H 18) Assign. A B Shift (ppm) 1. 26 0. 88 89. 56 MHz (CDCl 3)

Isopentane (C 5 H 12) Assign. Shift (ppm) A B C D 1. 447 1. 20 0. 869 0. 865 J(B, D)=7. 3 HZ. J(A, C)=6. 6 HZ. J(A, B)=6. 6 HZ 89. 56 MHz (CDCl 3)

2 -Propanol (C 3 H 8 O) Assign. Shift (ppm) A B C 4. 008 2. 16 1. 200 89. 56 MHz (CDCl 3)

3 -Chloro-1 -propanol (C 3 H 7 Cl. O) Assign. Shift (ppm) A B C D 3. 808 3. 683 2. 19 2. 017 89. 56 MHz (CDCl 3)

Chloroethylene (C 2 H 3 Cl) Assign. Shift (ppm) A 5. 396 B 5. 480 C 6. 264 J(A, B)= -1. 44 Hz J(A, C)= 7. 48 Hz J(B, C)=14. 46 Hz 300 MHz (CCl 4)

Styrene (C 8 H 8) Assign. Shift (ppm) A B C D 7. 50 to 7. 10 6. 692 5. 737 5. 225 86. 59 MHz (CDCl 3)

p-Xylene (C 8 H 10) Assign Shift (ppm) A B 2. 296 7. 046 300 MHz (CDCl 3)

2 -Bromo-p-xylene (C 8 H 9 Br) Assign. Shift (ppm) A B C D E 7. 34 7. 06 6. 99 2. 33 2. 27 89. 56 MHz (CDCl 3)

Ethyl acetate (C 4 H 8 O 2) Assign. Shift (ppm) A 4. 119 B 2. 038 C 1. 260 J(A, C)=7. 1 HZ. 89. 56 MHz (CDCl 3)

Butyraldehyde (C 4 H 8 O) Assign. Shift (ppm) A B C D 9. 764 2. 37 1. 64 0. 97 89. 56 MHz (CDCl 3)

1 -Hexyne (C 6 H 10) Assign. Shift (ppm) A B C D E 2. 18 1. 931 1. 52 1. 41 0. 92 89. 56 MHz (CDCl 3)

Butylamine (C 4 H 11 N) Assign. Shift (ppm) A B C D E 2. 680 1. 77 1. 43 1. 33 0. 92 89. 56 MHz (CDCl 3)

Benzoic acid (C 7 H 6 O 2) Assign. Shift (ppm) A B C D 12. 09 8. 12 7. 62 7. 45 89. 56 MHz (CDCl 3)

13 C NMR

Hexane (C 6 H 14 ) ppm 31. 87 22. 89 14. 16 Int. Assign. 1000 834 943 1 2 3 25. 16 MHz (CDCl 3)

Octane (C 8 H 18 ) ppm Int. 32. 15 29. 54 22. 88 14. 16 1000 960 881 642 Assign. 1 2 3 4 25. 16 MHz (CDCl 3)

Cyclohexane (C 6 H 12 ) ppm Int. 27. 10 1000 Assign. 1 25. 16 MHz (CDCl 3)

Toluene (C 7 H 8) ppm Int. 137. 83 214 129. 09 910 128. 28 1000 125. 38 517 21. 41 209 Assign. 1 2 3 4 5 25. 16 MHz (CDCl 3)

p-Xylene (C 8 H 10) ppm 134. 66 128. 97 20. 90 Int. Assign. 239 1000 229 3 2 1 25. 16 MHz (CDCl 3)

o-Xylene (C 8 H 10) ppm Int. 136. 42 383 129. 63 960 125. 85 1000 19. 66 587 Assign. 4 3 2 1 25. 16 MHz (CDCl 3)

m-Xylene (C 8 H 10) ppm Int. 137. 74 547 129. 96 423 128. 21 473 126. 13 1000 21. 31 403 Assign. 5 4 3 2 1 25. 16 MHz (CDCl 3)

Ethyl acetate (C 4 H 8 O 2) ppm Int. 171. 08 527 60. 44 1000 21. 00 571 14. 28 857 Assign. 4 3 2 1 15. 09 MHz (CDCl 3)

Cyclopentanone (C 5 H 8 O) ppm Int. Assign. 220. 16 146 38. 31 888 23. 31 1000 1 2 3 25. 16 MHz (CDCl 3)

Benzoic acid (C 7 H 6 O 2) ppm Int. 172. 77 287 133. 83 485 130. 28 980 129. 44 277 128. 49 1000 Assign. 1 2 3 4 5 25. 16 MHz (CDCl 3)

p-Bromoaniline (C 6 H 6 Br. N ) ppm Int. 145. 48 233 131. 93 1000 116. 70 925 110. 03 226 Assign. 4 3 2 1 25. 16 MHz (CDCl 3)

Diethyl ether (C 4 H 10 O) ppm Int. Assign. 65. 97 675 15. 35 1000 1 2 25. 16 MHz (CDCl 3)